Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Vinyl isocyanate → HCID 12573482, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Vinyl isocyanate | HCID 77094 | — |
| 반응물 | (1-Chloroethyl)carbamyl chloride | HCID 12573467 | — |
| 용매 | 1-Chloronaphthalene | HCID 7003 | — |
| 생성물 | Vinyl isocyanate | HCID 77094 | 8% |
| 생성물 | HCID 12573482 | HCID 12573482 | 92% |
반응 단계
30 parts of 1-chloroethylcarbamyl chloride are dissolved in 100 parts by volume of 1-chloronaphthalene and a solution of 16 parts of vinyl isocyanate in 20 parts by volume of 1-chloronaphthalene is added to the mixture in the course of 0.3 hour at 2° C. 12.5 parts (8% of theory) of vinyl isocyanate and 43 parts (92% of theory) of 1-chloroethyl isocyanate are obtained, the determinations being carried out by gas chromatography.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04411752 |
| 출처 데이터셋 | uspto-grants-1983_10 |
| ORD ID | ord-15907a3c4348420e97db91a68b610441 |
| 출처 메모 | uspto-grants-1983_10 |