Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → 6-(2-Chlorophenyl)-3-(4-oxopiperidino)-1,2,4-triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | Piperonylamine | HCID 2723901 | — |
| 반응물 | 3-Chloro-6-(o-chlorophenyl)-1,2,4-triazine | HCID 12581288 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 6-(2-Chlorophenyl)-3-(4-oxopiperidino)-1,2,4-triazine | HCID 13605527 | — |
반응 단계
1.5 g of 3-chloro-6-(2-chlorophenyl)-1,2,4-triazine, 3.05 g of piperidin-4-one monohydrate hydrochloride and 3.1 g of sodium carbonate are heated under reflux in 100 ml of ethanol for 4 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04613603 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-bde75dd99363429981065e3c265be9d8 |
| 출처 메모 | uspto-grants-1986_09 |