참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Butylimidazole | HCID 61347 | — |
| 반응물 | 1-(3-Bromopropyl)-4-methoxybenzene | HCID 12776996 | — |
| 생성물 | HCID 178448559 | HCID 178448559 | — |
반응 단계
A mixture of 2.5 g (0.02 mole) of 1-butyl-1H-imidazole and 4.61 g (0.02 mole) of 1-(3-bromopropyl)-4-methoxybenzene is heated at 140° C. for about 1.5 hours. Follow the progress of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5). At the completion of the reaction, the cooled reaction product is triturated thoroughly with ether and on drying, provides the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04613609 |
|---|
| 출처 데이터셋 | uspto-grants-1986_09 |
|---|
| ORD ID | ord-d17fe45ddae24492a2764b6e70704cee |
|---|
| 출처 메모 | uspto-grants-1986_09 |
|---|
