참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Allyl Alcohol | HCID 7858 | — |
| 반응물 | 1-(3,3-Dimethylcyclohexyl)ethanone | HCID 91388 | — |
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 생성물 | 1-(3,3-Dimethylcyclohexyl)-pent-4-en-1-one | HCID 6453423 | — |
반응 단계
Into a 2 liter autoclave is placed 700 grams of the diethyl ketal of 1-acetyl-3,3-dimethyl cyclohexane prepared according to Example II; 360 grams of allyl alcohol; and 10 grams of sodium acetate. The autoclave is sealed and heated to 150° C. and maintained at that temperature for a period of five hours. At the end of the five hour period, the autoclave is opened and the contents are filtered, washed with water and distilled on a 12" Goodloe column yielding the following fractions:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04613706 |
|---|
| 출처 데이터셋 | uspto-grants-1986_09 |
|---|
| ORD ID | ord-856fadf20ec64632964600cd02c6adba |
|---|
| 출처 메모 | uspto-grants-1986_09 |
|---|
