Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-6-nitroquinoline → 2-Methylquinolin-6-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-6-nitroquinoline | HCID 69172 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Methylquinolin-6-amine | HCID 103148 | — |
반응 단계
2-Methyl-6-nitroquinoline (18.8 g) was stirred under a hydrogen atmosphere at 206.8 kPa (30 p.s.i.) for 2 hours in ethanol solution containing 5% Pd/C. The catalyst was then removed by filtration, the filtrate evaporated to small volume in vacuo, and the resultant precipitate collected by filtration, washed with ethanol and ether, and dried to give the title compound, yield 13.2 g, m.p. 188°-189°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05130334 |
| 출처 데이터셋 | uspto-grants-1992_07 |
| ORD ID | ord-7b80bff0d19e477ba3aab3e969f15905 |
| 출처 메모 | uspto-grants-1992_07 |