Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydroxy-4-nitrobenzyl alcohol → 2-Hydroxy-4-nitrobenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydroxy-4-nitrobenzyl alcohol | HCID 11816094 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 2-Hydroxy-4-nitrobenzaldehyde | HCID 75570 | — |
반응 단계
6.0 g (35.5 mmol) of 2-(hydroxymethyl)-5-nitrophenol and 3.1 g (35.5 mmol) of activated manganese (IV) oxide in 100 ml of chloroform are heated under reflux for 20 h. The mixture is filtered through kieselguhr, concentrated and dried under high vacuum. The title compound is directly reacted further.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08076355B2 |
| 출처 데이터셋 | uspto-grants-2011_12 |
| ORD ID | ord-560a73694b2f4253913d518ae869b9b5 |
| 출처 메모 | uspto-grants-2011_12 |