Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → 5-Benzylidenehydantoin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Hydantoin | HCID 10006 | — |
| 반응물 | Ammonium formate | HCID 2723923 | — |
| 생성물 | 5-Benzylidenehydantoin | HCID 97857 | 91.9% |
반응 단계
A mixture of 100 grams (1.0 mole) of hydantoin, 106 grams (1.0 mole) of benzaldehyde, 63 grams (1.0 mole) of ammonium formate, and 230 grams (5.0 moles) of formic acid were held for 3 hours at reflux temperature. After the cooling off, there were obtained 173 grams of 5-benzylidene hydantoin, corresponding to 92% of theory based on hydantoin.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04345072 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-b37aacc2f732407fb601b0a860bba435 |
| 출처 메모 | uspto-grants-1982_08 |