Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
cis-4-(3-Chlorophenyl)-but-3-enylamine → 4-(3-Chlorophenyl)butan-1-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | cis-4-(3-Chlorophenyl)-but-3-enylamine | HCID 58679830 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Platinum dioxide monohydrate | HCID 11139377 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-(3-Chlorophenyl)butan-1-amine | HCID 10655071 | 74.2% |
반응 단계
A solution of cis-4-(3-chlorophenyl)-but-3-enylamine (1.2 g) in 20 mL methanol was added to platinum(IV) oxide monohydrate (0.12 g). The mixture was stirred under 1 atm of hydrogen for 16 h. The mixture was filtered through celite, and the methanol was removed in vacuo to yield 0.9 g of 4-(3-chlorophenyl)-butylamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07084154B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-6eda0c359052479e89b251fa31711b9d |
| 출처 메모 | uspto-grants-2006_08 |