Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → HCID 178482500, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 3-(Trifluoromethyl)benzoyl chloride | HCID 75257 | — |
| 반응물 | N-Methylhydrazinecarbothioamide | HCID 2723853 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 178482500 | HCID 178482500 | — |
반응 단계
A 42 g. portion of 4-methylthiosemicarbazide was reacted with 200 ml. of acetone, and then with 32 g. of pyridine and 83.6 g. of 3-trifluoromethylbenzoyl chloride. The mixture was worked-up as described in Example 1 to obtain 77.5 g. of the desired product, m.p. 111°-115°, after recrystallization from nitromethane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04346225 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-bd0437614152434bb4e32c1135ec93de |
| 출처 메모 | uspto-grants-1982_08 |