Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Octyn-3-ol, 3,6-dimethyl- → 3,6-Dimethyl-oct-1-en-3-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Octyn-3-ol, 3,6-dimethyl- | HCID 174244 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 촉매 | Zinc | HCID 23994 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3,6-Dimethyl-oct-1-en-3-ol | HCID 20526739 | — |
반응 단계
154 g (1 mole) of 3,6-dimethyl-oct-1-yn-3ol are dissolved in 100 ml of methanol, 1 g of an 0.1% strength palladium/calcium carbonate catalyst, which has been poisoned with zinc ions, is added, and hydrogen is passed in at 20° C. under atmospheric pressure. The hydrogenation is complete in 6 hours, when about 24 liters of hydrogen have been absorbed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04347388 |
| 출처 데이터셋 | uspto-grants-1982_08 |
| ORD ID | ord-a7393b65dacd4364838b740a4c2e917c |
| 출처 메모 | uspto-grants-1982_08 |