Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Amino-3-chloropyridazine → [2-(6-Chloro-3-pyridazinyl)-2-azavinyl]dimethylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Amino-3-chloropyridazine | HCID 21643 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | [2-(6-Chloro-3-pyridazinyl)-2-azavinyl]dimethylamine | HCID 6802247 | — |
반응 단계
A mixture of 3-amino-6-chloropyridazine (6.39 g, 49.3 mmol) and N,N-dimethylformamide dimethyl acetal (7.67 mL, 54.3 mmol) was stirred under reflux for 75 min. Excess N,N-dimethyl-formamide dimethyl acetal was removed to afford the title compound as a beige solid (tR 1.0 min (conditions 1), MH+=185).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822468B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-b23567cd310b4b37811b6c274507ad7a |
| 출처 메모 | uspto-grants-2014_09 |