Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromo-4-fluoroaniline → HCID 178505119, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromo-4-fluoroaniline | HCID 2779286 | — |
| 반응물 | N'-hydroxy-4-[2-(methanesulfonamido)ethylamino]-1,2,5-oxadiazole-3-carboximidamide | HCID 178505117 | — |
| 생성물 | HCID 178505119 | HCID 178505119 | — |
반응 단계
The title compound was prepared according to the procedure of Example 17 step E, using N-hydroxy-4-({2-[(methylsulfonyl)amino]ethyl}amino)-1,2,5-oxadiazole-3-carboximidamide and 3-bromo-4-fluoroaniline [Oakwood Products, Inc., product #013091] as the starting materials. LCMS for C12H15BrFN6O4S (M+H)+: m/z=437.0, 439.0. 1H NMR (400 MHz, DMSO-d6): δ 11.49 (s, 1H), 8.90 (s, 1H), 7.17 (m, 2H), 7.09 (dd, J=6.3, 2.5 Hz, 1H), 6.26 (t, J=6.1 Hz, 1H), 3.33 (m, 2H), 3.13 (q, J=6.0 Hz, 2H), 2.89 (s, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822511B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-8f452db05bf64b3a89c22a21330afe6f |
| 출처 메모 | uspto-grants-2014_09 |