Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Lithium Hydroxide → 3-Amino-6-(2,6-difluorophenyl)-5-fluoropicolinic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Lithium Hydroxide | HCID 3939 | — |
| 반응물 | Methyl 3-amino-6-(2,6-difluorophenyl)-5-fluoropicolinate | HCID 59226608 | — |
| 생성물 | 3-Amino-6-(2,6-difluorophenyl)-5-fluoropicolinic acid | HCID 59226513 | 79% |
반응 단계
Method 2 was followed using methyl 3-amino-6-(2,6-difluorophenyl)-5-fluoropicolinate (1.0 equiv.) and LiOH (1.0 equiv.) to give 3-amino-6-(2,6-difluorophenyl)-5-fluoropicolinic acid in 79% yield. LCMS (m/z): 269.0 (MH+), Rt=0.79 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09173883B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-95d3ce60c9904ca19a3455f175a064d9 |
| 출처 메모 | uspto-grants-2015_11 |