Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexane → Chloramben-methyl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | Chloramben | HCID 8630 | — |
| 반응물 | Trimethylsilyldiazomethane | HCID 167693 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | Chloramben-methyl | HCID 23714 | — |
반응 단계
206 mg (1.0 mmol) of 2,5-Dichloro-3-aminobenzoic acid was dissolved in 4 mL of acetone. 0.7 mL (1.4 mmol) of A hexane solution of 2.0M trimethylsilyldiazomethane was added thereto and stirred at room temperature for 1.5 hours. A solvent was removed to obtain methyl 2,5-dichloro-3-aminobenzoate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09174932B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-1cfcecd5fdcd4c12abcdfff6406355ba |
| 출처 메모 | uspto-grants-2015_11 |