Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoylhydrazine → N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoylhydrazine | HCID 11955 | — |
| 반응물 | Benzeneacetic acid, hydrazide | HCID 70301 | — |
| 반응물 | HCID 64393851 | HCID 64393851 | — |
| 생성물 | N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide | HCID 67153966 | 65% |
반응 단계
Following the procedure as described in Preparation 13, making variations as required to replace benzohydrazide with 2-phenylacetohydrazide to react with 2-benzamidoisonicotinic acid, N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide was obtained in 65% yield: MS (ES+) m/z 374.9 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09187426B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-041b11ff412e435fbd512076e40afaa5 |
| 출처 메모 | uspto-grants-2015_11 |