Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoromethanesulfonic acid, lithium salt → HCID 86610082, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoromethanesulfonic acid, lithium salt | HCID 3664839 | — |
| 반응물 | Methyl (2R)-2-oxiranecarboxylate | HCID 9877347 | — |
| 반응물 | 6-amino-4-fluoro-3-isopropyl-1,3-benzoxazol-2(3H)-one | HCID 68489676 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 86610082 | HCID 86610082 | — |
반응 단계
Prepared from 6-amino-4-fluoro-3-isopropyl-1,3-benzoxazol-2(3H)-one (Step 2, 0.77 g, 3.66 mmol), methyl (2R)-glycidate (0.374 g, 3.66 mmol) and lithium trifluoromethanesulfonate (0.57 g, 3.66 mmol) in acetonitrile (10 ml) according to the method of EXAMPLE 86, Step 8 (0.89 g, 78%); MS for C14H17FN2O5 m/z 313 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07141588B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-fb5eb590bec74a94bacda0376685cdca |
| 출처 메모 | uspto-grants-2006_11 |