Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 732287생성일: 2026년 10월 24일
1H-Indole-5-Carboxylic Acid → 6,11-dihydro-5H-diindolo[2,3-a:2',3'-c]carbazole-2,9,14-tricarboxylic acid
https://huagongshe.com/ko/reaction/732287
참여 물질
| 역할 | 이름 | HCID | 투입량 |
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| 반응물 | 1H-Indole-5-Carboxylic Acid | HCID 74280 | — |
| 용매 | Sulfuric acid methanol | HCID 18363649 | — |
| 생성물 | 6,11-dihydro-5H-diindolo[2,3-a:2',3'-c]carbazole-2,9,14-tricarboxylic acid | HCID 23240068 | 94.6% |
반응 단계
1.07 g of the indole-5-carboxylic acid trimer synthesized in Example 12 was suspended in 30 ml of 10% aqueous sulfuric acid-methanol solution, and the suspension was agitated for 2 hours at the temperature of 25° C. The suspension was suction-filtered with a perforated funnel, washed with methanol and dried to obtain 1.00 g of 6,11-dihydro-5H-diindolo [2,3-a:2′,3′-c] carbazole-2,9,14-tricarboxylic acid (indole-5-carboxylic acid trimer) with a light green color. The resultant trimer was pressure-molded with a tablet molding machine and the mold was cut into a piece with the diameter of 10 mm and thickness of 1 mm. A conductivity thereof was measured by the four terminal method and found to be 0.55 S/cm. The result of elemental analysis was: <C9.00H4.90N1.09O1.98Cl0.03(SO4)0.12>3.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07585981B2 |
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| 출처 데이터셋 | uspto-grants-2009_09 |
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| ORD ID | ord-b66d97e64f3946f496f6647493e4fd3e |
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| 출처 메모 | uspto-grants-2009_09 |
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