Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Chloro-4-nitrophenol → [2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Chloro-4-nitrophenol | HCID 10283 | — |
| 반응물 | 1-Chloro-2-(diethylamine)ethane hydrochloride | HCID 13363 | — |
| 용매 | Dichloromethane methanol | HCID 21226129 | — |
| 생성물 | [2-(3-Chloro-4-nitrophenoxy)ethyl]diethylamine | HCID 68816613 | — |
반응 단계
Prepared analogously to Example 4.1.a. from 3-chloro-4-nitrophenol and (2-chloroethyl)diethylamine hydrochloride. Yield: 1.25 g (79.5% of theory); C12H17ClN2O3 (M=272.73); calc.: molecular ion peak (M+H)+: 273/275; found: molecular ion peak (M+H)+: 273/275; Rf value: 0.44 (silica gel, dichloromethane/methanol (90:10)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07592373B2 |
| 출처 데이터셋 | uspto-grants-2009_09 |
| ORD ID | ord-0b2845645be14f609260747be85b6098 |
| 출처 메모 | uspto-grants-2009_09 |