Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroacetyl chloride → HCID 178448916, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroacetyl chloride | HCID 6577 | — |
| 반응물 | 2,3-Dimethylaniline | HCID 6893 | — |
| 반응물 | Butyl Isothiocyanate | HCID 11613 | — |
| 생성물 | HCID 178448916 | HCID 178448916 | — |
반응 단계
2-[(Z)-n-butylimino]-3-(2,3-dimethylphenyl)-thiazolidin-4-one is prepared following Method B and starting from 2,3-dimethylaniline, chloroacetyl chloride and n-butyl-isothiocyanate. LC-MS: tR=0.80 min, [M+1]+=277, 1H NMR (CDCl3): δ 7.23-7.16 (m, 2H), 6.99-6.94 (m, 1H), 4.01 (s, 2H), 3.38-3.23 (m, 2H), 2.33 (s, 3H), 2.05 (s, 3H), 1.59-1.49 (m, 2H), 1.38-1.25 (m, 2H), 0.91 (t, J=7.0 Hz, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | USRE045174E1 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-0413d746d0f540beb398a7a65c809f5e |
| 출처 메모 | uspto-grants-2014_09 |