Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroacetyl chloride → HCID 178457011, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroacetyl chloride | HCID 6577 | — |
| 반응물 | Cyclohexylamine | HCID 7965 | — |
| 반응물 | Isopropyl Isothiocyanate | HCID 75263 | — |
| 생성물 | HCID 178457011 | HCID 178457011 | — |
반응 단계
3-Cyclohexyl-2-[(Z)-isopropylimino]-thiazolidin-4-one is prepared starting from cyclohexylamine, chloroacetyl chloride and isopropylisothiocyanate following Method B. LC-MS: tR=0.83 min, [M+1]+=241, 1H NMR (CDCl3): δ 4.30 (tt, J=3.6, 12.0 Hz, 1H), 3.69 (s, 2H), 3.37 (hep, J=6.4 Hz, 1H), 2.40-2.25 (m, 2H), 1.84-1.75 (m, 2H), 1.64-1.50 (m, 2H), 1.40-1.20 (m, 4H), 1.14 (d, J=6.4 Hz, 6H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | USRE045174E1 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-a02decf412a843569f254b5a4c6b1db5 |
| 출처 메모 | uspto-grants-2014_09 |