Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromine → HCID 178524767, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | HCID 178418479 | HCID 178418479 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178524767 | HCID 178524767 | 82% |
반응 단계
Bromine (3.6 mL, 70.5 mmol) was added dropwise to a suspension of 6-Hydroxy-nicotinic acid (7 g, 50.32 mmol) in water (70 mL) at 00° C. and the mixture was stirred at room temperature for 4 hours. The precipitated solid was filtered, washed with cold water and dried to get the title compound as off white solid in 82% yield, 9 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846698B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-1169c5edf7c74bc9a8a658c183330218 |
| 출처 메모 | uspto-grants-2014_09 |