Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenol → (+)-4-(2-Methyldecanoyl) phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | Decanoic acid, 2-methyl- | HCID 91167 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | (+)-4-(2-Methyldecanoyl) phenol | HCID 53900693 | 40% |
반응 단계
Then, the same procedure as in Example 1 was repeated except that the above (+)-2-methyl decanoic acid was used instead of (+)-2-methyl butanoic acid to convert this compound into an acid chloride, which was reacted with phenol through aluminum chloride in methylene chloride to obtain (+)-4-(2-methyldecanoyl) phenol having the aforementioned physical and chemical properties at a yield of 40%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05137653 |
| 출처 데이터셋 | uspto-grants-1992_08 |
| ORD ID | ord-7f0319ed762c4c32be7fbb428e598d7f |
| 출처 메모 | uspto-grants-1992_08 |