Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorotrimethylsilane → 3,8-Dioxa-2,9-disiladecane, 2,2,9,9-tetramethyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | 1,4-Butanediol | HCID 8064 | — |
| 촉매 | Hexadecyltributylphosphonium bromide | HCID 84716 | — |
| 생성물 | 3,8-Dioxa-2,9-disiladecane, 2,2,9,9-tetramethyl- | HCID 140321 | — |
반응 단계
1 mole of butane-1,4-diol, 3 moles of trimethylchlorosilane and 0.002 moles of tributyl-hexadecyl phosphonium bromide were reacted at the reflux temperature (56°-96° C.) as in Example 1. The product was worked up by fractional distillation.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05142081 |
| 출처 데이터셋 | uspto-grants-1992_08 |
| ORD ID | ord-9db4bfcea3d94061a42271e73442d436 |
| 출처 메모 | uspto-grants-1992_08 |