Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butylamine → Phenyl n-butylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butylamine | HCID 8007 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Phenyl n-butylcarbamate | HCID 97513 | 71.97% |
반응 단계
n-Butylamine (4.9 ml, 50 mmol) was used for the same reaction as in Production Example 310-1, and purification was performed by silica gel column chromatography (hexane:ethyl acetate=4:1) to obtain the title compound (8.11 g, 41.97 mmol, 71.97%) as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07253286B2 |
| 출처 데이터셋 | uspto-grants-2007_08 |
| ORD ID | ord-51ba7a6db04e4598b99e8c14f289b527 |
| 출처 메모 | uspto-grants-2007_08 |