Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methyl-1-butene → ethyl 7-(3-methylbutyl)-2-(trifluoromethyl)-2H-chromene-3-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methyl-1-butene | HCID 11239 | — |
| 반응물 | ethyl 7-iodo-2-(trifluoromethyl)-2H-chromene-3-carboxylate | HCID 69517680 | — |
| 생성물 | ethyl 7-(3-methylbutyl)-2-(trifluoromethyl)-2H-chromene-3-carboxylate | HCID 69518920 | — |
반응 단계
The ester from Example 9a, Step 2 was coupled and using a similar protocol as described in Example 611d, Step 1 using the appropriate substitution of 3-methylbut-1-ene (77%): ESLRMS m/z 343.1 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07259266B2 |
| 출처 데이터셋 | uspto-grants-2007_08 |
| ORD ID | ord-66807ae13e854cdd8030895bf5808e80 |
| 출처 메모 | uspto-grants-2007_08 |