Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | HCID 178453037 | HCID 178453037 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt | HCID 178479178 | — |
반응 단계
Hydrogen chloride gas was bubbled through a 0° C. solution of tert-butyl 2-(1H-pyrazol-3-yl)benzylcarbamate (60 mg, 0.220 mmol) in ethyl acetate (5 ml) for 2 min and stirred for 40 min. A precipitate formed, and the suspension was concentrated in vacuo to give 2-(1H-pyrazol-3-yl)-benzylamine hydrochloride salt; MS (ES+) M+1 174.1 for C10H11N3.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07144899B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-22a5083e6e1a44fdb08b7e75ca87b653 |
| 출처 메모 | uspto-grants-2006_12 |