Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → HCID 46261794, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 3-Methoxyaniline | HCID 10824 | — |
| 반응물 | 4,6-dichloro-1-methyl-1H-pyrazolo(3,4-d)pyrimidine | HCID 222247 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 46261794 | HCID 46261794 | — |
반응 단계
m-Anisidine (1.1 eq) was added to a solution of 4,6-dichloro-1-methyl-1H-pyrazolo[3,4-d]pyrimidine 5 (1 eq.) and triethylamine (NEt3, 1.5 eq) in ethanol. The mixture was stirred at room temperature for 2 hr and then ether was added. The solid was filtered off and the filtrate concentrated in vacuo to give 6-chloro-N-(3-methoxyphenyl)-1-methyl-1H-pyrazolo[3,4-d]pyrimidin-4-amine 6.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08987280B2 |
| 출처 데이터셋 | uspto-grants-2015_03 |
| ORD ID | ord-80e6685e623640debceec97824a5680b |
| 출처 메모 | uspto-grants-2015_03 |