Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → 1-Isobutyl-3-methylthiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | Isobutyl isothiocyanate | HCID 68960 | — |
| 생성물 | 1-Isobutyl-3-methylthiourea | HCID 15568243 | 98.2% |
반응 단계
Methylamine (2M in methanol, 20.0 mL, 40.2 mmol) was added dropwise to isobutylisothiocyanate (2.00 mL, 16.5 mmol) during 15 minutes at room temperature. The reaction mixture was heated to reflux for 3.5 h and the solvent was evaporated off to give the title compound (2.37 g, 98%) as a colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08236951B2 |
| 출처 데이터셋 | uspto-grants-2012_08 |
| ORD ID | ord-a009c415bc374a209f29a2f4261b069c |
| 출처 메모 | uspto-grants-2012_08 |