Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine hydrate (1:1) → HCID 135697913, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | (4-Methoxyphenyl)ethanimidamide--hydrogen chloride (1/1) | HCID 12203394 | — |
| 반응물 | Ethyl 3-acetamido-2-oxobutanoate | HCID 22245807 | — |
| 생성물 | HCID 135697913 | HCID 135697913 | — |
반응 단계
Analogously to Example 7A, 5.1 g (25.4 mmol) of 2-(4-methoxyphenyl)ethanamidine hydrochloride (Example 4A) are reacted with 1.53 g (30.5 mmol) of hydrazine hydrate and 7.14 g (38.1 mol) of ethyl 3-(acetylamino)-2-oxobutanoate (Example 6A) to give N-{1-[3-(4-methoxybenzyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]ethyl}acetamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06998402B2 |
| 출처 데이터셋 | uspto-grants-2006_02 |
| ORD ID | ord-77ceaf58325a4be4b408ff2d4a5ca463 |
| 출처 메모 | uspto-grants-2006_02 |