Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aluminum bromide → 4-(4-fluorophenoxy)-5-[4-(methylsulfonyl)phenyl]-3(2H)-pyridazinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aluminum bromide | HCID 24409 | — |
| 반응물 | 2-Benzyl-4-(4-fluorophenoxy)-5-[4-(methylsulfonyl)phenyl]-3(2H)-pyridazinone | HCID 9846581 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 4-(4-fluorophenoxy)-5-[4-(methylsulfonyl)phenyl]-3(2H)-pyridazinone | HCID 21934162 | — |
반응 단계
The title compound was prepared by treating 2-benzyl-4-(4-fluorophenoxy)-5-[4-(methylsulfonyl)phenyl]-3(2H)-pyridazinone (Example 75) with AlBr3 in toluene according to the procedure in Example 11 (yield: 1.8 g, 95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07001895B2 |
| 출처 데이터셋 | uspto-grants-2006_02 |
| ORD ID | ord-e87118ab7853444f87dda44a2479da3a |
| 출처 메모 | uspto-grants-2006_02 |