Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Dibenzofuran-2-yloxy)-1-nitrobenzene → 4-(Dibenzofuran-2-yloxy)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Dibenzofuran-2-yloxy)-1-nitrobenzene | HCID 2102893 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 4-(Dibenzofuran-2-yloxy)aniline | HCID 66977456 | — |
반응 단계
The nitro intermediate (10 mmol) obtained above was dissolved in EtOAc (50 mL) and hydrogenated in the presence of 10% Pd/C (360 mg) until completion according to General Procedure H, as indicated by TLC or HPLC. The reaction mixture was then filtered to remove the catalyst. The solvent was removed in vacuuo to afford the desired 4-(dibenzofuran-2-yloxy)aniline, which was used directly for further transformation without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07361678B2 |
| 출처 데이터셋 | uspto-grants-2008_04 |
| ORD ID | ord-91c3553133314f1daa44a78be95675db |
| 출처 메모 | uspto-grants-2008_04 |