Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloro-p-phenylenediamine sulfate → Tetraethyl-{(2-chloro-p-phenylene)bis [imino(thiocarbonyl)]}diphosphoramidate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloro-p-phenylenediamine sulfate | HCID 22584 | — |
| 반응물 | 1-[Ethoxy(isothiocyanato)phosphoryl]oxyethane | HCID 556832 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Tetraethyl-{(2-chloro-p-phenylene)bis [imino(thiocarbonyl)]}diphosphoramidate | HCID 131711916 | — |
반응 단계
Employing the process of Example 1 in every detail except that 2-chloro-p-phenylenediamine sulfate is neutralized and allowed to react with two equivalents of diethyl phosphoroisothiocyanatidate ##STR7## in chloroform instead of methylene chloride to afford the title compound, m.p. 148°-149° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04229383 |
| 출처 데이터셋 | uspto-grants-1980_10 |
| ORD ID | ord-3362b68d456942cc830fca9d641d07de |
| 출처 메모 | uspto-grants-1980_10 |