Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Ethylpiperidin-3-one hydrochloride → HCID 19694168, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Ethylpiperidin-3-one hydrochloride | HCID 433439 | — |
| 반응물 | 1-Benzyl-4-chloro-1H-imidazo[4,5-c]pyridine | HCID 14199152 | — |
| 생성물 | HCID 19694168 | HCID 19694168 | — |
반응 단계
Following the procedure of Example 13 and using 1-benzyl-4-chloro-1H-imidazo[4,5-c]pyridine (0.60 g, 2.5 mmol) and (0.36 g, 2.8 mmol) of N-ethyl-3-piperidone gave the free base of the title compound which was purified by flash chromatography on silica gel eluting with EtOAc to give, after preparation of the salt, the dihydrochloride, 0.59 hydrate as an amorphous solid, 0.30 g (26%):
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723468 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-ba5fcf5d0a3744acbef08bc1f8e5f3b4 |
| 출처 메모 | uspto-grants-1998_03 |