Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2,3-Benzothiadiazole-5-carboxylic acid → N-(4-chloro-3-(pyridin-2-yl)phenyl)benzo[d][1,2,3]thiadiazole-5-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2,3-Benzothiadiazole-5-carboxylic acid | HCID 2735458 | — |
| 반응물 | 4-Chloro-3-(pyridin-2-yl)aniline | HCID 40151925 | — |
| 생성물 | N-(4-chloro-3-(pyridin-2-yl)phenyl)benzo[d][1,2,3]thiadiazole-5-carboxamide | HCID 58614738 | — |
반응 단계
50 mg of 4-chloro-3-(pyridin-2-yl)aniline was coupled to benzo-1,2,3-thiadiazole-5-carboxylic acid via Procedure G. The crude product was purified via reverse phase HPLC to yield N-(4-chloro-3-(pyridin-2-yl)phenyl)benzo[d][1,2,3]thiadiazole-5-carboxamide. MS (Q1) 367 (M)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09278961B2 |
| 출처 데이터셋 | uspto-grants-2016_03 |
| ORD ID | ord-24b7fcfce10f4a0eb6922c5576869c72 |
| 출처 메모 | uspto-grants-2016_03 |