Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorodiisopropylphosphine → N1-(2-isopropyl-6-methylphenyl)-N2-(diisopropyl-phosphino)-4-methylbenzamidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorodiisopropylphosphine | HCID 538967 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 반응물 | HCID 178425631 | HCID 178425631 | — |
| 생성물 | N1-(2-isopropyl-6-methylphenyl)-N2-(diisopropyl-phosphino)-4-methylbenzamidine | HCID 178425661 | — |
반응 단계
Procedure as described for NP Amidine I using the following amounts: 1.33 g of N1-(2-isopropyl-6-methylphenyl)-4-methylbenzamidine (Amidine V, 5.0 mmol), 2.50 mL of 2.0 M butyllithium (5.0 mmol), 0.80 mL chlorodiisopropylphosphine (5.0 mmol). After filtration to remove lithium chloride and removal of solvent, a yellow semi-solid was isolated (1.86 g, 97%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09283555B2 |
| 출처 데이터셋 | uspto-grants-2016_03 |
| ORD ID | ord-0dc94fc71bc24b18b415f2c8fc3d938c |
| 출처 메모 | uspto-grants-2016_03 |