Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorosulfonic acid → Ethyl 2-(4-(chlorosulfonyl)-2-ethylphenoxy)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorosulfonic acid | HCID 24638 | — |
| 반응물 | Ethyl (2-ethylphenoxy)acetate | HCID 21986411 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Ethyl 2-(4-(chlorosulfonyl)-2-ethylphenoxy)acetate | HCID 21986343 | — |
반응 단계
A solution of crude ethyl(2-ethylphenoxy)acetate (intermediate 107) in chloroform (6 ml) was stirred with chlorosulfonic acid (1.33 ml) at ambient temperature for 4 hours. The reaction mixture was quenched by the addition of ice and the organic mixture separated by using a hydrophobic frit. The title compound was isolated by evaporation of this filtrate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07091237B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-1f39594965174048aec2d27ed501f246 |
| 출처 메모 | uspto-grants-2006_08 |