Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178507362, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Lithium aluminum hydride | HCID 28112 | — |
| 반응물 | 5-nitro-1H-indazole-3-carboxylic Acid | HCID 7144652 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 178507362 | HCID 178507362 | 19.9% |
반응 단계
5-nitro-1H-indazole-3-carboxylic acid (500 mg, 0.002 mol) was dissolved in 50 mL THF, added lithium tetrahydroaluminate (366 mg, 0.00964 mol) in 3 portions and stirred at room temperature overnight. 65 mg (15%). Water (366 μL), 15% NaOH solution (366 μL), and water (1.1 mL) were added cautiously and the mixtured was filtered. The filtrate was concentrated under vacuum to give the product (65 mg, 15%) as an oil. m/z=160.0.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07312233B2 |
| 출처 데이터셋 | uspto-grants-2007_12 |
| ORD ID | ord-620f4c73f84141379fb79a07e6e77db7 |
| 출처 메모 | uspto-grants-2007_12 |