Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Isocyanate → HCID 178485940, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Isocyanate | HCID 12228 | — |
| 반응물 | HCID 178433288 | HCID 178433288 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 178485940 | HCID 178485940 | 58.8% |
반응 단계
A mixture of 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole (5.1 g.) and methyl isocyanate (2.0 g.) in acetonitrile was heated for 18 hours in a pressure vessel at 100°. After cooling, the solid obtained was collected and recrystallised from isopropyl alcohol-acetonitrile to give N-methyl-N'-[2-((4-methyl-5-imidazolyl)methylthio)ethyl]urea (4.0 g.) m.p. 158°-159°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04053473 |
| 출처 데이터셋 | uspto-grants-1977_10 |
| ORD ID | ord-9ca53a86750742b4af26748847283b7b |
| 출처 메모 | uspto-grants-1977_10 |