Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 19989021, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Bis(3-aminopropyl)amine | HCID 5942 | — |
| 반응물 | Tert-butyldicarbonate | HCID 22064466 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 19989021 | HCID 19989021 | 44.7% |
반응 단계
A solution of 33 g of tert-butyl dicarbonate in 200 ml of methylene chloride was added at 5° C. to a solution of 39.3 g of 3,3'-diaminodipropylamine in 300 ml of methylene chloride and after stirringf or 16 hours at 20° C., water was added, followed by decanting and evaporation to dryness. The residue was chromatographed on silica (eluant; methanol-ammonia (98-2)) to obtain 15.5 g of the expected product which was used as is for the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05064861 |
| 출처 데이터셋 | uspto-grants-1991_11 |
| ORD ID | ord-9d3134bdfaae4dde982fa1a852abdee2 |
| 출처 메모 | uspto-grants-1991_11 |