Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Allyl-N-(1,1-dimethoxyprop-2-yl)-urethane → Ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Allyl-N-(1,1-dimethoxyprop-2-yl)-urethane | HCID 15069988 | — |
| 용매 | Formic Acid | HCID 284 | — |
| 생성물 | Ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate | HCID 15069993 | — |
반응 단계
76.5 g (0.213 mol) of 64.5% pure N-allyl-N-(1,1-dimethoxyprop-2-yl)-urethane are heated in 180 ml of formic acid at 100° C. for one hour. The mixture is poured into ice-water and extracted with CH2Cl2, the extracts are washed neutral with NaHCO3 solution, dried over MgSO4 and concentrated and the residue is distilled.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04990517 |
| 출처 데이터셋 | uspto-grants-1991_02 |
| ORD ID | ord-726ffd53130b44d89bbbee4ac9d7de60 |
| 출처 메모 | uspto-grants-1991_02 |