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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 982140생성일: 2026년 10월 24일

Methyl 3-amino-2-thiophenecarboxylate → HCID 178437764, 화합물

https://huagongshe.com/ko/reaction/982140

반응식

참여 물질

역할이름HCID투입량
반응물Methyl 3-amino-2-thiophenecarboxylateHCID 89652—
반응물Propionamidine hydrochlorideHCID 415117—
생성물HCID 178437764HCID 178437764—

반응 조건

온도60 °C

반응 단계

Methyl 3-amino-2-thiophenecarboxylate (4.67 g,) and propionamidine (3 g, were combined and heated in an oil both for 1/2 hour at 60° C.; 1/2 hour at 80° C.; 1/2 hour at 100° C. and finally for 4 hours at 120° C. The mixture was cooled, triturated with ether, filtered and washed with ether to obtain 0.67 g of the product; m.p. 233°-237° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04994464
출처 데이터셋uspto-grants-1991_02
ORD IDord-b46f55dfb744492280886387eb3267fb
출처 메모uspto-grants-1991_02