Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Dinitroadamantane → 1-Amino-3-nitroadamantane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Dinitroadamantane | HCID 583950 | — |
| 촉매 | Nickel | HCID 935 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 1-Amino-3-nitroadamantane | HCID 18410483 | 80% |
반응 단계
The reaction was effected in the same manner as Example 65 except for using Raney nickel (5 mole % of Ni relative to a substrate) instead of 5% Pd-C and that reacting for 4 hours. The conversion of 1,3-dinitroadamantane was 99%, and 1-amino-3-nitroadamantane (yield 80%) was formed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06468487B1 |
| 출처 데이터셋 | uspto-grants-2002_10 |
| ORD ID | ord-321fca3a1c2d4b3d8076f12075741850 |
| 출처 메모 | uspto-grants-2002_10 |