Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Hydroxyphenyl)diphenylsulfonium chloride → (p-Hydroxyphenyl)diphenylsulfonium trifluoromethanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Hydroxyphenyl)diphenylsulfonium chloride | HCID 18411308 | — |
| 반응물 | Potassium Trifluoromethanesulfonate | HCID 23664779 | — |
| 생성물 | (p-Hydroxyphenyl)diphenylsulfonium trifluoromethanesulfonate | HCID 22389942 | — |
반응 단계
To an aqueous solution of 11.5 g of the diphenyl-4-hydroxyphenylsulfonium chloride, 22 g of an aqueous 37.5% potassium trifluoromethanesulfonate solution was dropwise added with stirring at room temperature to obtain a white precipitate. The white precipitate was filtered, and then the impurities were washed with distilled water several times, followed by drying under reduced pressure to obtain 10.7 g of the desired diphenyl-4-hydroxyphenylsulfonium trifluoromethanesulfonate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06468714B2 |
| 출처 데이터셋 | uspto-grants-2002_10 |
| ORD ID | ord-687c6ba1df6a4c13b38b4937adaba582 |
| 출처 메모 | uspto-grants-2002_10 |