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HRID1024458

反应详情

EQUATION

反应方程式

HRID 1024458 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1ccc(C(=O)Cl)cc1
HCID74372

Benzoyl chloride, 4-(1,1-dimethylethyl)-

C11H13ClO

结构：COC(=O)C(C(C)C)N(C)C(=O)c1ncc(-c2ccc([N+](=O)[O-])cc2)s1
HCID67150337

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C(C(C)C)N(C)C(=O)c1ncc(-c2ccc(NC(=O)c3ccc(C(C)(C)C)cc3)cc2)s1
HCID52935706

未命名化合物

收率 56%

PROCEDURE

实验过程

The title compound was synthesized analogous to Example 27, using 4-tert-butylbenzoyl chloride and intermediate 4. Yield: 56%; 1H NMR (DMSO-d6, 300 MHz): δ 10.38 (s, 1H), 8.37 (s, 1H), 8.04 (m, 4H), 7.78 (d, 2H), 7.57 (d, 2H), 6.27-4.76 (d, 1H), 3.69 (s, 3H), 3.47-2.95 (s, 3H), 2.35 (m, 1H), 1.33 (s, 9H), 1.11 (bs, 3H), 0.90 (bs, 3H); MS (ESI): m/z 508.2 [M+H]+.