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HRID1182869

反应详情

EQUATION

反应方程式

HRID 1182869 的结构方程式

REACTANTS

反应物

2
结构：Cl.Cl.NO[C@@H]1CCNC1
HCID66713918

未命名化合物

结构：CC1(C)C(=O)CC[C@]2(C)[C@H]3CC[C@]4(C)[C@@H](O)CC[C@H]4[C@@H]3CC[C@@]12O
HCID68729176

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)/C(=N/O[C@@H]2CCNC2)CC[C@]2(C)[C@H]3CC[C@]4(C)[C@@H](O)CC[C@H]4[C@@H]3CC[C@@]12O.Cl
HCID87573863

未命名化合物

PROCEDURE

实验过程

The title compound was obtained in 51% yield following the procedure described in Example 2 and starting from 4,4-dimethyl-5α,17β-dihydroxyandrostan-3-one (Preparation 28, 33 mg) and 3-(R)-pyrrolidinyloxyamine dihydrochloride (Preparation 12, 69 mg). The crude product was triturated with Et2O and the resulting precipitate was filtered to give the title compound I-by.

WORKUP

后处理

  1. customThe crude product was triturated with Et2O
  2. filtrationthe resulting precipitate was filtered