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HRID1256705

反应详情

EQUATION

反应方程式

HRID 1256705 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(C=S)cc1
HCID18177535

未命名化合物

结构：CCOC(=O)c1c(C)c(C)c(C(=O)C=Cc2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)c(O)c1OC
HCID86599973

未命名化合物

2 次

PRODUCTS

生成物

1
结构：COc1c(O)c(C(=O)C=Cc2cc(C)cs2)c(C)c(C)c1C(=O)O
HCID86599977

未命名化合物

PROCEDURE

实验过程

This compound was synthesized from 2′-hydroxy-4′-ethyloxycarbonyldimethylmethyloxyacetophenone (starting material 1) and 4-methylthiobenzaldehyde according to general method 2 described earlier. Purification was by chromatography on silica gel (elution: cyclohexane/ethyl acetate 9/1) followed by preparative HPLC (reverse phase RP18, Licrospher 12 μm, elution: water/methanol/trifluoroacetic acid: 22/78/0.3).

WORKUP

后处理

  1. customPurification
  2. washfollowed by preparative HPLC (reverse phase RP18, Licrospher 12 μm, elution: water/methanol/trifluoroacetic acid: 22/78/0.3)