HRID1368952

反应详情

EQUATION

反应方程式

HRID 1368952 的结构方程式

PROCEDURE

实验过程

is prepared by using the method described in the example 4e starting from 1-{4-[2-(2-benzyloxyethoxy)ethoxy]phenyl}-2-phenyl-4-(tetrahydropyran-2-yloxy)butan-1-one (10 g, 19.2 mmol) and 3-(tetrahydropyran-2-yloxy)phenyl bromide (9.8 g, 38 mmol). The product is purified by flash chromatography with toluene-methanol (50:1) as eluent. Yield 5.7 g, 43%.

WORKUP

后处理

  1. customis prepared
  2. customThe product is purified by flash chromatography with toluene-methanol (50:1) as eluent