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HRID1475996

反应详情

EQUATION

反应方程式

HRID 1475996 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NO
HCID97534

tert-Butyl N-hydroxycarbamate

C5H11NO3

结构：C[C@H](C(=O)O)N(C)C(=O)OC(C)(C)C
HCID16211306

N-(tert-Butoxycarbonyl)-N-methyl-D-alanine

C9H17NO4

PRODUCTS

生成物

1
结构：C[C@H](C(=O)ONC(=O)OC(C)(C)C)N(C)C(=O)OC(C)(C)C
HCID86654175

未命名化合物

PROCEDURE

实验过程

[(tert-Butoxy)carbonyl]amino (2R)-2-{[(tert-butoxy)carbonyl](methyl)amino}propanoate is prepared from (2R)-2-{[(tert-butoxy)carbonyl](methyl)amino}propanoic acid and N-tert-butoxycarbonyl hydroxylamine according to Scheme 6. The compound exists as rotomers and is reported as such. (0.95 g, 60%), 1H NMR (500 MHz, CHLOROFORM-d) δ ppm 7.81-7.95 (1H, m), 4.60-5.04 (1H, m), 2.85-2.93 (3H, m), 1.40-1.54 (18H, m), 1.22-1.33 (3H, m).