huagongshe.com
HRID1486707

反应详情

EQUATION

反应方程式

HRID 1486707 的结构方程式

REACTANTS

反应物

3
结构：Cc1c(C=O)cccc1[N+](=O)[O-]
HCID262241

2-methyl-3-nitrobenzaldehyde

C8H7NO3

结构：CC(C)(C)NC(=O)C1CCNCC1
HCID7175833

未命名化合物

结构：Cc1c(CN2CCC(C(=O)NC(C)(C)C)CC2)cccc1[N+](=O)[O-]
HCID86706542

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(N)cccc1CN1CCC(C(=O)NC(C)(C)C)CC1
HCID86706541

未命名化合物

PROCEDURE

实验过程

The title compound is prepared according to the reactions described for BB-5 above starting from 2-methyl-3-nitro-benzaldehyde and piperidine-4-carboxylic acid tert-butylamide yielding after reductive amination 1-(2-methyl-3-nitro-benzyl)-piperidine-4-carboxylic acid tert-butylamide; LC-MS A: tR=0.62 min; [M+H]+=334.32 followed by reduction with stannous chloride the title compound; LC-MS A: tR=0.45 min; [M+H]+=304.32.

WORKUP

后处理

  1. customThe title compound is prepared