HRID1527372

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8857

Ethyl acetate

C4H8O2

结构：CC(C)(C)OC(=O)N1C[C@@H]2C[C@@H]2[C@H]1C(=O)N[C@H](CO)c1cccc(Cl)c1F

HCID68283613

未命名化合物

PRODUCTS

生成物

结构：COC[C@@H](NC(=O)[C@@H]1[C@H]2C[C@H]2CN1C(=O)OC(C)(C)C)c1cccc(Cl)c1F

HCID68284071

未命名化合物

PROCEDURE

实验过程

was prepared according to Scheme B9 (Step B) from (1S,2S,5R)-2-[(S)-1-(3-chloro-2-fluoro-phenyl)-2-hydroxy-ethylcarbamoyl]-3-aza-bicyclo[3.1.0]hexane-3-carboxylic acid tert-butyl ester. TLC, Rf (EtOAc): 0.65; MS (UPLC/MS): 413.4/415.4 [M+H]+, 457.4/459.4 [M+HCOO]−; tR (HPLC conditions a): 3.67 min.

WORKUP

后处理

customwas prepared
custom3.67 min.